The comparative analysis of the solid-state ~(31)P NMR spectra of Re-Pt vinylidene complexes

机译：Re-Pt亚乙烯基复合物的固态〜（31）P NMR光谱的对比分析

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The two vinylidene complexes Cp(CO)_2RePt(μ-C=CHPh)(PPh_3)(CO) and Cp(CO)_2RePt(μ-C=CHPh)(PPh_3)_2 and their precursors PPh3 and P(PPh_3)_4 were studied by solid-state nuclear magnetic resonance. We analysed ~(31)P cross-polarization spectra acquired in static conditions and with magic angle spinning. The chemical shift tensors of each sample were determined by fitting their spectra using SIMPSON simulations.

机译：两偏二乙烯基复合物CP（CO）_2 _2REPT（μ-C = CHPH）（PPH_3）（CO）和CP（CO）_2 _2 _2 _2（μ-C = CHPH）（PPH_3）_2及其前体PPH3和P（PPH_3）_4 由固态核磁共振研究。我们分析了在静态条件下获得的〜（31）的次偏振光谱和魔法角旋转。通过使用SIMPSON模拟拟合它们的光谱来确定每个样品的化学移位张量。

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《International Conference on Applied Physics, Information Technologies and Engineering》|2020年|p1-807|共5页
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K T Smolyarov; N V Volkov; A N Matsulev; A A Kondrasenko;
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The comparative analysis of the solid-state ~(31)P NMR spectra of Re-Pt vinylidene complexes

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