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Synthesis and Characterization of Graphene/Cu2SnS3 Quantum Dots Composites

机译:石墨烯/ CU2SNS3量子点复合材料的合成与表征

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In this paper,employing graphite oxide (GO),CuCl,SnCl4·5H2O and dimethyl sulfoxide (DMSO) as raw materials,the composites of graphene/Cu2SnS3 quantum dots (QDs) were prepared simply and quickly using the hydrothermal method.Meanwhile,the separate Cu2SnS3 QDs were also synthesized in the same way.The as-obtained Cu2SnS3 QDs and composites' phase structures were analyzed and characterized by powder X-ray diffraction (XRD),and the results indicated that the size of the Cu2SnS3 QDs in the composites were less than that of the separate Cu2SnS3 QDs.At the same time,their morphologies were also observed and cross-confirmed by Transmission Electron Microscopy (TEM),and the measurements manifested that Cu2SnS3 QDs were uniformly dispersed on the surface of the graphene,while the separate Cu2SnS3 QDs have obvious glomeration.In addition to this,elemental analysis was also made to verify the existence of Cu2SnS3 on the surface of graphene.
机译:在本文中,使用石墨氧化物(GO),CuCl,SnCl4·5H 2 O和二甲基亚砜(DMSO)作为原料,制备石墨烯/ Cu2Sns3量子点(QDS)的复合材料,简单迅速使用水热法。偶尔,单独的Cu2SNS3 QD也以相同的方式合成。通过粉末X射线衍射(XRD)分析和表征作为获得的Cu2SNS 3 QD和复合材料的相结构,结果表明Cu2SNS3 QD在复合材料中的尺寸同时少于单独的Cu2SNS3 QDS.AT,还观察到它们的形态并通过透射电子显微镜(TEM)交叉证实,并且测量表明CU2SNS3QD均匀地分散在石墨烯表面上单独的Cu2SNS3 QD具有明显的幽默。除此之外,还进行了元素分析以验证石墨烯表面上的Cu2SNS3的存在。

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