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Nanorods/Nanostructral Vanadium Oxide Prepared by Spray Pyrolysis

机译:喷雾热解制备的纳米棒/纳米结构钒氧化物

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Nanorods/nanostructural vanadium oxide thin film was prepared on glass substrates by Spray Pyrolysis technique at a substrate temperature of 450°C. The precursor solution was obtained by 0.1 M concentrations of VC1_3 in de-ionize water. The structural, optical and morphological properties of this thin film was investigated by means of UV-vis spectrophotometer, X-ray diffraction (XRD), atomic-force microscopy (AFM) and scanning electron microscope (SEM). The optical result show that the optical gap is equal to 2.38 eV. The structural investigation conducted by X-ray diffraction showed that V_5O_9 thin film was polycrystalline with anorthic structure. SEM and AFM images revealed the formation of interconnected nanorods.
机译:通过在450℃的底物温度下喷雾热解技术在玻璃基板上制备纳米棒/纳米结构氧化物薄膜。前体溶液通过0.1M浓度的VC1_3在去电离水中获得。通过UV-Vis分光光度计,X射线衍射(XRD),原子力显微镜(AFM)和扫描电子显微镜(SEM)研究了该薄膜的结构,光学和形态学性质。光学结果表明光学间隙等于2.38eV。由X射线衍射进行的结构研究表明,V_5O_9薄膜是具有高兴结构的多晶。 SEM和AFM图像揭示了互连纳米棒的形成。

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