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Optimization synthesis of porous carbon by solid phase method and its adsorption performance on tetracycline

机译:通过固相法优化多孔碳的合成及其对四环素的吸附性能

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In this work, the porous carbon was synthesized by a solid phase method, using phenolic resin as carbon precursor and F127 as template. The obtained materials were characterized by Fourier Transform Infrared Spectroscopy (FT-IR), X-Ray Diffraction (XRD), Transmission Electron Microscopy (TEM), and N_2 adsorption-desorption isotherms. The adsorption performances of porous carbon were investigated by adsorbing tetracycline. The experimental part design optimization of the tetracycline adsorption rate of the complete solid phase synthesis of porous carbon material conditions of carbon materials with porous. The optimum conditions for the synthesis of the porous carbon were systematically investigated. Results indicated that the optimum synthesized conditions obtained in the experimental analysis were a raw material ratio of 1:3 (in phenolic resin: F127 = 1:3), stable curing of 5 h at 200 °C and carbonization 2 h at 900 °C.
机译:在这项工作中,使用固相法合成多孔碳,使用酚醛树脂作为碳前体和F127作为模板。通过傅里叶变换红外光谱(FT-IR),X射线衍射(XRD),透射电子显微镜(TEM)和N_2吸附 - 解吸等温线,其特征在于傅里叶变换的材料。通过吸附四环素研究多孔碳的吸附性能。实验部设计优化碳材料多孔碳材料条件完全固相合成的四环素吸附速率。系统地研究了合成多孔碳的最佳条件。结果表明,实验分析中获得的最佳合成条件是原料比为1:3(在酚醛树脂:F127 = 1:3),在200℃下稳定固化5小时,碳化2小时900℃ 。

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