首页> 外文会议>International Conference on Chemistry and Material Science >Characterization Studies of Cyclotron CS-30 Carbon Puller Material Using Powder X-Ray Diffraction and SEM, EDX Cross Section Method
【24h】

Characterization Studies of Cyclotron CS-30 Carbon Puller Material Using Powder X-Ray Diffraction and SEM, EDX Cross Section Method

机译:用粉末X射线衍射和SEM,EDX横截面法对回旋加速器CS-30碳拉米材料的表征研究

获取原文

摘要

The carbon puller material of Cyclotron CS-30 has been characterized to investigate the structure and composition of the puller. Two samples of pullers have been prepared in the form of powder from locally made carbon and the original cyclotron puller. X-ray diffraction (XRD) analysis of both samples powder gives identification of the structure and phase type of carbon, meanwhile the morphology and the elemental composition of both samples can be shown by Scanning Electron Microscopy (SEM) and Energy Dispersive X-Ray Analysis (EDX) technique. XRD samples are prepared by grinding the puller surface meanwhile the samples for SEM analysis are prepared by cross section method. XRD result shows amorphous carbon structure and a typical broad XRD profile's peaks and the diffused nature of the XRD profile indicate the presence of disorder in the samples. The first peak of the profile corresponds to the (002) peak of the hexagonal graphite structure, while the second peak corresponds to the (100) and (101) for both samples. Results of SEM-EDX showed that the carbon material from the original default puller of the CS-30 cyclotron contains mass percentage of lead significantly by 9.15%.
机译:回旋加速器CS-30的碳牵引材料已经表征研究了拉拔器的结构和组成。已经以来自局部制造的碳和原始回旋器拉皮器的粉末的形式制备了两种拉拔器样品。两种样品粉末的X射线衍射(XRD)分析给出了结构和相类型的碳的鉴定,同时可以通过扫描电子显微镜(SEM)和能量分散X射线分析来示出两种样品的形态和元素组成(EDX)技术。同时通过横截面法制备SEM分析的样品来制备XRD样品。通过横截面方法制备SEM分析的样品。 XRD结果显示非晶碳结构和典型的广泛XRD型峰值和XRD型材的扩散性质表明样品中存在病症。轮廓的第一峰值对应于六边形石墨结构的(002)峰值,而第二峰值对应于两个样本的(100)和(101)。 SEM-EDX的结果表明,来自CS-30循环的原始默认拉拔器的碳材料含有9.15%的铅的质量百分比。

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号