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Optimization of Rotational Speed for Growing BaFe_(12)O_(19) Thin Films using Spin Coating

机译:使用旋涂的生长Bafe_(12)O_(19)薄膜的转速优化

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Barium ferrite (BaFe~(12)O_(19), BaM) thin films were fabricated by the spin coating of precursors obtained by using a sol-gel method. The effects of the rotational speed on the spin-coating process for growing a BaM thin film were investigated in this study. Coated films were heat-deposited at different rotational speeds ranging from 2000 to 4000 rpm, while the number of layers was set to nine. Further, the effect of the number of layers on the growth of BaM thin films was discussed. For this purpose, we take the layers number 1 to 12 and take the constant rotational speed of 3000 rpm. All the film were characterized using X-Ray diffraction, Scanning Electron microscope, and Energy-dispersive X-Ray spectroscopy and Vibrating Sample Magnetometer. It was found that by increasing the rotational speed the amount of material deposited on the Si substrate decreased. The measured grain size of the BaM thin film was nearly similar for three three different rotational speeds. However, the grain size was found to increase the number of layers.
机译:通过使用溶胶 - 凝胶法得到的前体的旋涂来制造钡铁氧体(Bafe〜(12)O_(19),BAM)薄膜。本研究研究了旋转速度对生长BAM薄膜的旋涂过程的影响。涂覆的薄膜以2000至4000rpm的不同转速热沉积,而层数设定为九个。此外,讨论了层数对BAM薄膜生长的影响。为此目的,我们将图层为1到12,并采用3000 rpm的恒定转速。所有薄膜使用X射线衍射,扫描电子显微镜和能量分散X射线光谱和振动样品仪。发现,通过增加旋转速度,沉积在Si衬底上的材料的量减少。对于三种三种不同的旋转速度,BAM薄膜的测量晶粒尺寸几乎相似。然而,发现晶粒尺寸增加了层数。

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