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Some Reflections On Styrene Suspension Polymerization Experiment Teaching

机译:关于苯乙烯悬浮聚合实验教学的几点思考

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The results of suspension polymerization of styrene were studied by changing the dosage of initiator, stirring speed, size of stirring paddle, content of dispersant and reaction temperature. The results showed that when using 500 ml four flasks, styrene 40 ml and polyvinyl alcohol solution (3 g polyvinyl alcohol dissolved in 1000 ml deionized water) 200 ml, initiator 0.5 g, stirring speed 300-450 r/min, temperature range 86-95°C, using the stepped heating method and using the impeller with a spreading blade diameter of 43 mm can ensure the success of the experiment, and the yield is relatively high.
机译:通过改变引发剂的剂量,搅拌速度,搅拌桨尺寸,分散剂和反应温度的含量来研究苯乙烯的悬浮聚合结果。结果表明,当使用500mL四瓶时,苯乙烯40mL和聚乙烯醇溶液(将3g聚乙烯醇溶解在1000ml去离子水中)200mL,引发剂0.5g,搅拌速度300-450 r / min,温度范围86- 95°C,使用阶梯式加热方法并使用叶片的叶片直径为43mm,可以确保实验的成功,产率相对较高。

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