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Experimental Estimation of the Elastic Modulus of Non-Hazardous Waste Incineration Bottom Ash Aggregates by Indentation Tests - Microanalysis of Particles by Scanning Electron Microscopy

机译:通过扫描电子显微镜通过缩进试验对非危险废物焚烧底灰聚集体的弹性模量的实验估计 - 扫描电子显微镜微量分析

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An original experimental campaign never conducted until now on Non-Hazardous Waste Incineration aggregates is presented in this paper. The experiments were conducted in two phases: Scanning Electron Microscopy (SEM) and instrumented indentation. A cartography followed by a series of Quantitative Chemical Microanalysis (QCM) was carried out on the 0/12.5 mm fraction of the particle size distribution. Instrumented indentation tests were carried out on isolated particles of 25 mm in diameter. Observations at the SEM yielded the exact chemical composition of the bottom ashes. It has been found that the proportions of the chemical elements composing the material are slightly different from those of other studies. This difference has made it possible to note that the zone of production of the bottom ash significantly influences their physicochemical characteristics. From the indentation curves obtained, the "Olivier and Pharr" method was used to determine the reduced modulus of elasticity "E_r". Mean values of approximately 65 GPa and 40 GPa were obtained respectively for vitreous phases and less vitreous ones.
机译:本文介绍了直到现在的非危险废物焚烧聚集体的原始实验活动。实验以两相进行:扫描电子显微镜(SEM)和仪表压痕。在粒度分布的0 / 12.5mm分数上进行了一系列定量化学微分分析(QCM)的制图。仪表化压痕试验在直径为25mm的分离的颗粒上进行。 SEM的观察结果产生了底部的精确化学成分。已经发现,构成材料的化学元素的比例与其他研究的比例略有不同。这种差异使得可以注意到底灰的生产区域显着影响其物理化学特性。从获得的压痕曲线,使用“橄榄糖和Pharr”方法来确定减少的弹性模量“e_r”。分别为玻璃阶段和贫玻璃体较低的玻璃体阶段获得约65GPa和40gPa的平均值。

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