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Preparation and Properties of Sr_2NaNb_50_(15) Lead-Free Piezoelectric Ceramics by Sol-Gel Method

机译:溶胶 - 凝胶法制备SR_2NANB_50_(15)无铅压电陶瓷的制备及性能

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Sr_2NaNb_5O_(15) ceramic powders have been synthesized by sol-gel method, ceramics were sintered via a pressureless sintering method. The effect of calcining temperature on the phase composition and microstructure of ceramic powders were investigated by TG-DSC, XRD and SEM analyses. The influence of sintering temperature on density, microstructure and properties of the ceramics were systematically analyzed. The results showed that the optimal calcining temperature was 1300°C, the average size of ceramic powders was about 3 urn. When the sintering temperature was 1300°C, the ceramics showed optimized densification and electrical properties(/7=4.663 g/cm~3, d_(33)=45 pC/N, 5=1126, tanδ0.027, E_c=17.91 kV/cm, P_r=6.72 |iC/cm~2, P_s=9.45 uC/cm~2)
机译:SR_2NANB_5O_(15)通过溶胶 - 凝胶法合成陶瓷粉末,通过无压烧结方法烧结陶瓷。通过TG-DSC,XRD和SEM分析研究了煅烧温度对陶瓷粉末相成分和微观结构的影响。系统地分析了烧结温度对陶瓷密度,微观结构和性能的影响。结果表明,最佳煅烧温度为1300℃,陶瓷粉末的平均尺寸约为3瓮。当烧结温度为1300℃时,陶瓷显示出优化的致密化和电性能(/7=4.663g / cm〜3,d_(33)= 45cc / n,5 = 1126,Tanδ0.027,e_c = 17.91 kV / cm,p_r = 6.72 | IC / cm〜2,p_s = 9.45 UC / cm〜2)

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