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Transesterification of Jatropha Oil to Biodiesel by Using Catalyst Containing Ca(C_3H_7O_3)_2 as a Solid Base Catalyst

机译:使用含Ca(C_3H_7O_3)_2作为固体碱催化剂的催化剂,通过催化剂酯交换到生物柴油中的酯交换

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An direct precipitation method of Calcium glyceroxide Ca(C_3H_7O_3)_2 was proposed. The prepared Ca(C_3H_7O_3)_2 was effective in transesterification of Jatropha oil into fatty acid methyl esters (FAME). The Ca(C_3H_7O_3)_2 catalysts were characterized by using XRD, solid state ~(13)C-NMR, FTIR, and Hammett indicator. The influence of various reaction variables on the conversion was investigated. Under a condition of methanol/oil molar ratio of 9:1, a catalyst amount of 4 wt%, reaction time of 1.5 h, and reaction temperature of 65°C, over 95% of biodiesel yield was obtained.
机译:提出了一种直接沉淀甘油钙(C_3H_7O_3)_2的沉淀方法。制备的Ca(C_3H_7O_3)_2在JATROPHA油的酯交换中有效,进入脂肪酸甲酯(FAME)。通过使用XRD,固态〜(13)C-NMR,FTIR和HAMMETT指示剂表征CA(C_3H_7O_3)_2催化剂。研究了各种反应变量对转化率的影响。在甲醇/油摩尔比为9:1的条件下,催化剂量为4wt%,反应时间为1.5小时,反应温度为65℃,得到超过95%的生物柴油产量。

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