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Solid base catalyst for producing biodiesel oil and method for producing the same, reactor and device for producing biodiesel oil, and method for producing biodiesel oil using the device
Solid base catalyst for producing biodiesel oil and method for producing the same, reactor and device for producing biodiesel oil, and method for producing biodiesel oil using the device
It is intended to provide a solid base catalyst by which biodiesel fuel (BDF) can be efficiently produced from a starting oil or fat originating in a plant, a method of producing the same, a reactor and an apparatus for producing BDF, and a method of producing BDF by using this apparatus. The solid base catalyst, which has a basic strength (H_) of 15 or higher and comprises calcium oxide having a base amount of 0.1 mmol/g or more, is produced by baking a starting material for the catalyst (for example, quick lime, calcium carbonate, calcium acetate, slaked lime, etc.) in an atmosphere having water and a gas being substantially free from carbon dioxide gas (for example, highly pure helium gas, a gas mixture of nitrogen with oxygen, etc.) at a temperature of 300SUPo/SUPC or higher. The reactor comprises an airtight container having a channel through which a fluid flows from one (inlet) side to the other (outlet) side. This reactor is packed with the above-described solid basic catalyst. It is preferred that the reactor is provided with blocking means at both ends so as to prevent the external air (in particular, carbon dioxide) from flowing thereinto.
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机译:本发明旨在提供一种固体基础催化剂,通过该固体基础催化剂可以有效地从源自植物的原料油或脂肪中生产生物柴油燃料(BDF),其生产方法,反应器和用于生产BDF的设备以及方法。使用该设备生产BDF的过程。通过烘烤催化剂的起始原料(例如生石灰,生石灰,硬石),制备具有15或更高的基本强度(H_)且包含碱含量为0.1mmol / g或更高的氧化钙的固体碱催化剂。碳酸钙,乙酸钙,熟石灰等)在温度为水和基本上不含二氧化碳的气体(例如,高纯氦气,氮气与氧气的气体混合物等)中的气氛中300 o SUP> C或更高。该反应器包括具有通道的气密容器,流体从该通道从一个(入口)侧流到另一(出口)侧。该反应器装有上述固体碱性催化剂。优选的是,反应器在两端设有阻挡装置,以防止外部空气(特别是二氧化碳)流入其中。
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