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Supercritical Carbon Dioxide Extraction of Volatile Compounds from Antarctic krill (Euphausia superha)

机译:南极磷虾(Euphausia Superha)的超临界二氧化碳提取挥发性化合物

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Supercritical carbon dioxide (SC-CO2) extraction and simultaneous distillation extraction (SDE) were used to determine the volatile composition of Antarctic krill (Euphausia superba). The optimal extraction conditions for the oils yield within the experimental range of variables examined were temperature 40 °C, pressure 60 MPa, and extraction time 150 min. The maximum measured extraction yield was 12.34 ± 0.20 %. The chemical composition of the volatile compounds was adsorpted and analyzed by headspace solid phase microextraction (HS-SPME) and gas chromatography/mass spectrometry (GC/MS), respectively. A total of 35 compounds were identified including 2 alcohols, 6 aldehydes, 1 ketone, 2 furans, 4 acids, 2 amines, 5 aromatic compounds, and 13 hydrocarbons.
机译:超临界二氧化碳(SC-CO2)提取和同时蒸馏萃取(SDE)用于确定南极磷虾(Euphausia SuperBa)的挥发性组成。在检查的变量的实验范围内的油产量的最佳提取条件为温度40℃,压力60MPa和150分钟的提取时间。最大测量的提取产率为12.34±0.20%。通过顶空固相微萃取(HS-SPME)和气相色谱/质谱(GC / MS),吸附并分析挥发性化合物的化学成分。共鉴定出35种化合物,包括2醇,6醛,1酮,2呋喃,4酸,2胺,5个芳族化合物和13个烃。

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