Synthesis of 2-hydroxyl-3-sulfonic acid sodium salt-propyl lacrylate

摘要

2-hydroxyl-3-sulfonic acid sodium salt-propyl lacrylate was synthesized through the three-step process (sulfonation, ring-closing reaction, and esterification) by using epichlorohydrin as the starting material. The structure of oxiranemethane sulfonic acid sodium salt and end product 2-hydroxyl-3-sulfonic acid sodium salt-propyl lacrylate was identified by FTIR and Melting point. The influence factors of the synthesis process were studied. The optimal condition of the synthesis of ring-closing reaction and esterification was gained. Through the synthesis method, a corresponding synthesis of lauric acid, 14 acid, palmitic acid, 18 acid were gained. Then they were on the surface tension tests to determine the critical micelle concentration.