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MICROSTRUCTURE CHARACTERIZATION ON SILICON CARBIDE FORMATION FROM NATURAL WOOD

机译:自然木材碳化硅形成的微观结构特征

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Dark red meranti and kapur, are two important types of wood in Malaysia were used as precursors to fabricate porous silicon carbide. A carbon template was produced by pyrolysis at 850°C in an oxygen free atmosphere. The carbon template was further subjected to infiltration process with silicon. The infiltration process was carried out in a tube furnace in argon flow at 1500°C with two different holding times; 2 hours and 3 hours. Thermo gravimetric analysis was done to investigate the decomposition behavior of the two species. The resulting silicon carbide was characterized by XRD. The formation of silicon carbide and also excess silicon were found. The microstructure was characterized by scanning electron microscope (SEM). An increase in holding time during infiltration increased the density as well as formation of silicon carbide (SiC). Dark red meranti precursor is likely suitable for production of silicon carbide compared to kapur due to the higher SiC.
机译:暗红色的Meranti和Kapur,是马来西亚的两种重要类型的木材被用作制造多孔碳化硅的前体。通过在850℃下在无氧气氛中热解产生碳模板。碳模板进一步用硅进行渗透过程。渗透过程在1500℃下在氩气流的管炉中进行,两个不同的保持时间; 2小时3小时。进行热重量分析以研究两种物种的分解行为。通过XRD表征得到的碳化硅。发现碳化硅的形成,也是过量的硅。通过扫描电子显微镜(SEM)的特征在于微观结构。在渗透期间的保持时间增加增加了密度以及碳化硅(SiC)的形成。与kapur相比,暗红色的Meranti前体可能适用于由于kapur而导致的碳化硅。

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