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Preparation and Characterization of CaCu_3Ti_4O_(12) Ceramics by Cold Isostatic Press Forming

机译:冷等静压压制成型Cacu_3Ti_4O_(12)陶瓷的制备与表征

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CaCu_3Ti_4O_(12) (CCTO) ceramics were prepared by cold isostatic press (CIP) forming combined with the conventional sintering method. The effects of calcining temperature on properties of CCTO ceramics were investigated. The dielectric properties as the function of temperature at typical frequencies were measured in the temperature range from 243 to 363 K. In addition, the dielectric properties and complex impedances at room temperature were analyzed in a frequency range from 20 Hz to 10~6 Hz. The results showed that CCTO ceramics with dielectric constant higher than 10~4 were obtained. Compared with the dry press forming, CCTO ceramics prepared by CIP had more homogeneous grains, less porosity and better dielectric properties.
机译:CACU_3TI_4O_(12)(CCTO)陶瓷由冷等静压压(CIP)与常规烧结法相结合制备。研究了煅烧温度对基于CCTO陶瓷性能的影响。作为典型频率的温度函数的电介质特性在243至363k的温度范围内测量。此外,在20Hz至10〜6Hz的频率范围内分析介电性质和复杂的阻抗。结果表明,获得具有高于10〜4的介电常数的基准陶瓷。与干压成型相比,CCTO通过CIP制备的陶瓷具有更均匀的晶粒,孔隙率较小,介电性能更高。

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