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Influence of oxidation of Ti particle during laser remelting process on the microstructure of laser remelted NiTi coatings

机译:激光重熔过程中Ti粒子氧化对激光重熔乳头涂层微观结构的影响

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Commercial available Ni and Ti powder were blended together and deposited on stainless steel by atmospheric plasma spray(APS). Subsequently the as-sprayed coatings were laser remelted with a Nd -YAG pulsed laser source. Cross-sections of as-sprayed and laser-remelted coatings were characterized by scanning electron microscopy (SEM). Prior to SEM observations, the laser remelted coatings were polished and etched by Kroll etchant. Meanwhile, the energy dispersive spectrometer (EDS) was employed to analyze the chemical distribution of the coating both as-sprayed and laser remelted. The results indicated that APS sprayed NiTi coatings presented a dense microstructure with Ni splats and Ti splats distributing uniformly. Oxygen partial pressure in the argon leads to the burning of Ti splats during the laser remelting process. And Ti oxides located at the bottom of the laser molten pool because of the laser stiffness and molten flow. Moreover, the top part of the molten pool mainly involved in Ni columnar grains.
机译:可商业的Ni和Ti粉末混合在一起并通过大气等离子体喷雾(AP)沉积在不锈钢上。随后用Nd-yag脉冲激光源重新熔化时喷涂涂层。通过扫描电子显微镜(SEM)以喷涂和激光重熔涂层的横截面。在SEM观察之前,通过Kroll蚀刻剂抛光激光重熔涂层并蚀刻。同时,采用能量分散光谱仪(EDS)分析喷涂和激光重熔涂层的化学分布。结果表明,APS喷涂NITI涂层呈含有Ni Splats和Ti Splats均匀分布的致密微观结构。在激光重熔过程中,氩气中的氧气分压导致Ti Splats的燃烧。由于激光刚度和熔融流动,位于激光熔池底部的Ti氧化物。此外,熔池的顶部主要涉及Ni柱状晶粒。

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