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SYNTHESIS AND HYDROLISIS CONDITION EXPLORATION OF TETRAMIDO SUBSTITUTED SINGLE NUCLEUS IRON PHTHALOCYANINE

机译:四脒取代的单核铁酞菁的合成与水解条件探索

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摘要

The trimellitic anhydride, urea, FeCl3, NH4Cl, as raw materials, ammonium molybdate as catalyst, and tetramido substituted single nucleus iron phthalocyanine was synthesized. Then the most optimum hydrolysis time of tetramido substituted single nucleus iron phthalocyanine was explored. Results revealed that the optimal hydrolysis reaction time was 1.5 h. And the methods of determining the content of mental and carboxyl in the hydrolysis were established.
机译:合成偏苯二酐,尿素,FECL3,NH 4 Cl,作为原料,钼酸铵作为催化剂,以及四脒取代的单核铁酞菁。然后探讨了四脒取代的单核铁酞菁的最佳水解时间。结果表明,最佳水解反应时间为1.5小时。确定确定水解中精神和羧基含量的方法。

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