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In-situ Analysis of the Chemical Vapor Synthesis of Nanocrystalline Silicon Carbide by Aerosol Mass Spectrometry

机译:气溶胶质谱法的纳米晶碳化硅化学蒸汽合成的原位分析

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An Aerosol Mass Spectrometer (AMS) is a combiantion of a Quadrupol-(QMS) and a Particle Mass Spectrometer (PMS) and enables the in-situ of gas phase processes for the generation of nanoparticles.Size distributions of ultrafinie silicon carbide particles in the range of 10~4 atomic mass units (amu) to 10~7 amu are measured in the PMS.Simultaneously,molecular species up to 300 amu can be detected in the QMS.Aerosols containing nanocrystalline silicon carbide are produced from tetramethylsilane (TMS) by thermal decomposition.In situ process analysis with the AMS as a function of process parameters was performed to elucidate the analysis with the AMS as a function of process parameters was performed to elucidate the formation and growth mechanisms of SiC nanoparticles.
机译:气溶胶质谱仪(AMS)是Quadrupol-(QMS)和颗粒质谱仪(PMS)的组合,使得能够原位的气相过程用于产生纳米颗粒。提高超薄碳化硅颗粒的分布在PMS中测量10〜4个原子质量单位(AMU)至10〜7 AMU的范围。可以在QMS中检测到高达300AMU的分子种类。含有纳米晶碳化硅的癸醇由四甲基硅烷(TMS)产生热分解。用AMS作为工艺参数的函数进行热分解,以阐明与AMS进行分析,因为进行过程参数以阐明SiC纳米粒子的形成和生长机制。

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