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The Photocatalytic Degradation of Methylene Blue Using Bismuth Vanadate (Bi_2VO_(5.5)) Powder

机译:使用钒酸铋(Bi_2VO_(5.5))粉末的光催化降解亚甲基蓝色

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Bismuth vanadate (Bi_2VO_(5.5)) powder has been successfully prepared by microwave method. Bismuth nitrate and ammonium vanadate were used as the starting precursors with the mole ratio of 2:1 in 2-propanol. The microwave power was 500 Watt for 2-6 min. The yellow powder was obtained and calcined at 500°C for 2h. The structure was identified by X-ray diffraction (XRD). The morphology was investigated by field emission scanning electron microscopy (FESEM). The chemical composition was determined by energy dispersive X-ray spectrometry (EDXS). The functional groups were investigated by fourier transform infrared spectrometry (FTIR). The photocatalytic degradation of methylene blue (MB) using Bi_2VO_(5.5) powder was studied by ultraviolet-visible spectrophotometry (UV-Vis).
机译:钒酸铋(Bi_2VO_(5.5))粉末已通过微波法成功制备。硝酸铋和钒酸铵用作摩尔比为2:1的起始前体在2-丙醇中。微波功率为500瓦,2-6分钟。得到黄色粉末并在500℃下煅烧2小时。通过X射线衍射(XRD)鉴定该结构。通过场发射扫描电子显微镜(FeSEM)研究了形态。通过能量分散X射线光谱法(EDXS)测定化学成分。通过傅里叶变换红外光谱法(FTIR)研究了官能团。通过紫外 - 可见分光光度法(UV-VI)研究了使用Bi_2VO_(5.5)粉末的光催化降解亚甲基蓝(MB)。

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