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Dispensing and Hermetic Sealing Rb in a Miniature Reference Cell for Integrated Atomic Clocks

机译:分配和隐蔽密封Rb在微型参考电池中的集成原子钟

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An innovative method for filling and sealing the reference cell for a Rubidium (Rb) integrated atomic clock is presented. We used a simple, low-temperature solder sealing technique for producing mini-cells of the size of 12x 10x2 mm, suitable for Rb miniature atomic clocks. The cell is made by two glass slides acting as the top and bottom walls, joined by a solder ring acting as the sidewall. In the frame of this research, we also developed a safe and convenient method for easily handling Rb: the alkali metal is stored inside a 'pool' of dodecane. which protects it from oxidation. Pure liquid Rb is then dispensed inside the cell using a glass micropipette; finally, the cell is heated in vacuum, in order to realize the sealing. The hermeticity achieved by the cell was tested by sealing N2O gas and monitoring its pressure through absorbance measurements using FTIR spectroscopy. The presented method allows easy handling and long-term storage of Rb, and finally led to the production of functional hermetic mini-cells.
机译:提出了一种填充和密封铷(RB)集成原子时钟参考电池的创新方法。我们使用了一种简单的低温焊接密封技术,用于生产12倍10x2 mm的尺寸的迷你细胞,适用于RB微型原子钟。电池由用作顶壁的两个玻璃载玻片制成,用作侧壁的焊点连接。在本研究的框架中,我们还开发了一种安全,方便的方法,可轻松处理RB:碱金属存储在十二烷的“游泳池”内。从氧化保护它。然后使用玻璃微型插脚在电池内部分配纯液体Rb;最后,将电池在真空中加热,以实现密封。通过使用FTIR光谱通过吸光度测量密封N2O气体并通过吸光度测量来测试细胞实现的气密性。呈现的方法允许易于处理和长期存储RB,最终导致功能性密封迷你细胞的产生。

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