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Effect of Drying Process on the Evaluation of Microstructure of Clays using Scanning Electron Microscope (SEM) and Mercury Intrusion Porosimetry (MIP)

机译:干燥过程对扫描电子显微镜(SEM)和汞侵入孔隙瘤(MIP)粘土微观结构评价的影响

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This research reviewed and investigated the effect of drying and specimen preparation method for micro-structural observation and pore size distribution measurement according to various soils and test conditions, in utilizing Scanning Electron Microscope(SEM) and Mercury Intrusion Porosimetry(MIP), the major instruments for microscopic studies. Different types of soils, such as slurry state specimen of extremely high water content and reconstituted specimen from Honmoku clay, and undisturbed soils of Ariake and Osaka Pleistocene clays were used. For drying these soils, three types of drying methods such as air, oven and freeze drying were adopted for comparison. Through examining these results, it has been known that inappropriate adoption of drying method may lead to unrighteous understanding on the microstructure of fine-grained soils and that however, different drying method to the same specimen can be adopted on occasions depending on test purposes.
机译:本研究综述并研究了根据各种土壤和试验条件的微观结构观察和孔径分布测量的干燥和样本制备方法的影响,利用扫描电子显微镜(SEM)和汞侵入孔隙瘤(MIP),主要仪器用于显微镜研究。使用不同类型的土壤,例如来自Honmoku粘土的极高含水量和重构标本的浆液状态标本,以及ariake和大阪全脲烯粘土的未受干扰的土壤。为了干燥这些土壤,采用三种类型的干燥方法,例如空气,烤箱和冷冻干燥。通过检查这些结果,已知干燥方法的不适当采用可能导致对细菌土壤的微观结构的不太理解,然而,可以根据测试目的,可以在偶尔采用不同的干燥方法到相同的样本。

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