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Inverse identification and microscopic estimation of parameters for models of sound absorption in porous ceramics

机译:多孔陶瓷吸音模型参数的逆识别和微观估计

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Samples of porous ceramics Al_2O_3, manufactured by a promising technology of gelcasting of cellural foams by using biopolymers as gel-formers, are examined in the impedance tube using the transfer function method. It is shown that the ceramics of total porosity around 90% forms an excellent sound absorbing material in the frequency range from 500 Hz to 6.4 kHz. Experimentally-determined curves of acoustic impedance and absorption are then used for inverse identification of relevant geometric parameters like: tortuosity, viscous and thermal permeability parameters and characteristic lengths. These parameters are required by some advanced models of sound propagation in rigid porous media, developed by Johnson, Koplik and Dashen, Champoux and Allard, with some variations introduced by Pride et al., and Lafarge et al. These models are utilized to produce curves of acoustic impedance and absorption that are used by the identification procedure which minimizes the objective function defined as a squared difference to the appropriate curves obtained experimentally. As a matter of fact, some experimental data are used for the determination of parameters while the other data - obtained for another sample of the same porous ceramics, yet having different thickness - serve for the validation purposes. Moreover, it is observed that the identified characteristic length for thermal effects corresponds very well to the average radius of pores, whereas the characteristic length for viscous forces is similar with the average size of "windows" linking the pores. The identification procedure minimises the objective function with respect to a set of some independent dimensionless parameters from which the actual model parameters can be calculated. In the definitions of the dimensionless parameters two reference frequencies are introduced - one relevant for viscous effects, the other for thermal effects. Such approach renders the optimization procedure very robust. In general, it is observed that, if the total porosity is known, simultaneous identification of the remaining model parameters is feasible by using only the objective function. In particular, the inverse identification allows to estimate the so-called static thermal permeability which in practice is not easy to determine by direct measurements, and thus, very often because of lack of this parameter, the simplified Lafarge model must be used which approximate this parameter with an analytical result obtained for a porous medium with circular cylindrical pores. Finally, a periodic microscopic cell consisting of a few pores representing an average morphology of porous ceramics is proposed and a finite-element analysis with periodic boundary conditions in order to estimate the static viscous permeability parameter is presented.
机译:多孔陶瓷Al_2O_3的样品通过使用生物聚合物作为凝胶成型剂,通过使用生物聚合物作为凝胶制品制造的通过使用生物聚合物制造,在阻抗管中使用转移函数方法检查。结果表明,90%约90%的总孔隙率的陶瓷在500Hz至6.4kHz的频率范围内形成优异的声音吸收材料。然后使用实验确定的声阻抗和吸收的曲线用于相反识别相关的几何参数,如:曲折,粘性和热渗透率参数和特征长度。这些参数是由刚性多孔介质中的一些高级声音传播模型,由Johnson,Koplik和Dashen,Champoux和Allard开发的,由Pride等人引入了一些变体。和Lafarge等人。这些模型用于产生声阻抗和吸收的曲线,该识别过程使用,该识别过程最小化定义为与实验获得的适当曲线的平方差异定义的目标函数。事实上,一些实验数据用于测定参数,而其他数据用于相同多孔陶瓷的另一个样品,但具有不同的厚度 - 用于验证目的。此外,观察到,识别的热效应的特征长度对孔的平均半径非常良好,而粘性力的特征长度与链接孔的“窗口”的平均尺寸相似。识别过程最小化关于一组关于一组一些独立的无量纲参数的目标函数,从中可以计算实际模型参数。在无量纲参数的定义中,引入了两种参考频率 - 与粘性效果相关,另一个用于热效应。这种方法呈现优化程序非常坚固。通常,观察到,如果已知总孔隙率,则通过仅使用目标函数即可同时识别剩余的模型参数。特别地,逆识别允许估计所谓的静态热渗透性,在实践中不易通过直接测量确定,因此,通常由于缺乏此参数,必须使用简化的Lafarge模型,其近似于这参数具有用于具有圆柱孔的多孔介质的分析结果。最后,提出了一种周期性的微观细胞,其由代表多孔陶瓷的平均形态的孔组成,并且具有周期性边界条件的有限元分析,以估计静态粘性渗透率参数。

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