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Synthesis of Gold Nanoparticles Using the Extract of Sedum praealtum and Its Deposition on a Ceramic Substrate

机译:景天提取物合成金纳米粒子及其在陶瓷基底上的沉积

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In the present research the synthesis of gold nanoparticles (AuNPs) was established using the extract of Sedum praealtum. It should be pointed out that the conditions of synthesis directly influence the size, morphology, stability and physicochemical properties of the nanoparticles obtained. The extract of the plant was characterized by FTIR spectroscopy finding groups N-H, C-OH, who are credited with the reducing capacity of the ions AU~(+3). The AuNP's obtained were characterized by UV-visible spectroscopy, observing plasmones absorbance between 530 and 550 nm characteristic of these nanoparticles, moreover they were characterized by SEM and was observed the nanometric sizes, the reduction capacity of the extract was evaluated by voltammetric study, observing the intervals of the processes of reducing and oxidation of the ionic species. Additionally, it was done the deposition of nanoparticles synthesized on a ceramic substrate in order to achieve its stabilization and then the nanocomposite was analyzed by SEM.
机译:在本研究中,使用景天景天提取物建立了金纳米颗粒(AuNPs)的合成。应当指出,合成条件直接影响所得纳米颗粒的尺寸,形态,稳定性和理化性质。通过FTIR光谱法对植物的提取物进行表征,发现N-H,C-OH基团,其归因于离子AU〜(+3)的还原能力。通过紫外-可见光谱对所得的AuNP进行表征,观察这些纳米颗粒在530-550nm之间的等离激元吸光度,此外,通过SEM对其进行表征并观察纳米尺寸,通过伏安法研究提取物的还原能力,观察离子种类的还原和氧化过程的间隔。另外,进行了在陶瓷基底上合成的纳米颗粒的沉积以实现其稳定,然后通过SEM分析纳米复合材料。

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