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Synthesis of Gold Nanoparticles Using the Extract of Sedum praealtum and Its Deposition on a Ceramic Substrate

机译:用Sedum Praealtum提取物合成金纳米粒子及其在陶瓷基材上的沉积

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In the present research the synthesis of gold nanoparticles (AuNPs) was established using the extract of Sedum praealtum. It should be pointed out that the conditions of synthesis directly influence the size, morphology, stability and physicochemical properties of the nanoparticles obtained. The extract of the plant was characterized by FTIR spectroscopy finding groups N-H, C-OH, who are credited with the reducing capacity of the ions AU~(+3). The AuNP's obtained were characterized by UV-visible spectroscopy, observing plasmones absorbance between 530 and 550 nm characteristic of these nanoparticles, moreover they were characterized by SEM and was observed the nanometric sizes, the reduction capacity of the extract was evaluated by voltammetric study, observing the intervals of the processes of reducing and oxidation of the ionic species. Additionally, it was done the deposition of nanoparticles synthesized on a ceramic substrate in order to achieve its stabilization and then the nanocomposite was analyzed by SEM.
机译:在本研究中,使用SEDUMPRAEALTUM的提取物建立金纳米颗粒(AUNP)的合成。应该指出的是,合成条件直接影响所获得的纳米颗粒的尺寸,形态,稳定性和物理化学性质。植物的提取物的特征在于FTIR光谱法发现N-H,C-OH,官能团被认为是Au〜(+3)的还原能力。所获得的AUNP的特征在于UV可见光谱,观察到这些纳米颗粒的530和550nm的特征在于530和550nm的吸光度,此外,通过SEM表征,观察到纳米尺寸,通过伏安的研究评估提取物的减少能力,观察。离子物质的还原和氧化过程的间隔。另外,在陶瓷基材上沉积合成的纳米颗粒以实现其稳定性,然后通过SEM分析纳米复合材料。

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