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Structural Characteristics and Morphological Studies of SnO2 Powder Sample Synthesized by Sol Gel Route

机译:Sol凝胶途径合成SnO 2 粉末样品的结构特征及形态学研究

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Wideband Tin oxide (SnO2) has drawn a great deal of attention due to its excellent properties in a gas sensing material, photovoltaic cells, fuel cells etc. In the present work SnO2 sample is synthesized by Sol-gel route. XRD study has been conducted for determination of crystallinity and the structure of SnO2 sample. The pattern gets indexed in Tetragonal phase and low-intensity XRD peaks (110) and (211) are noticeable, indicating that the crystallization of the SnO2 sample powder is underway from the amorphous state. Debye Scherer's (DS) formula is used for the estimation of the particle size. The morphological analysis of the sample is carried out by TEM (Carl Zeiss make Model No. EVO18). TEM micrograph has demonstrated that the particles are integrated together to form largely sized agglomerates.
机译:宽带氧化锡(SNO 2 )由于其在当前工作中的气体传感材料,光伏电池,燃料电池等中的优异性能,因此引起了大量的注意力 2 样品由溶胶 - 凝胶途径合成。已经进行了XRD研究,以确定结晶度和SnO结构 2 样本。在四边形相位和低强度XRD峰(110)和(211)中被索引,表明SNO的结晶表示 2 从非晶态开始样品粉末。 Debye Scherer(DS)配方用于估计粒径。样品的形态学分析通过TEM进行(Carl Zeiss Make No. Evo18)。 TEM显微照片已经证明颗粒集成在一起以形成大小的尺寸附聚物。

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