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Characterization of nanostructured dendritic silver bismuth sulfide produced by solvothermal reactions

机译:溶剂热反应制备的纳米树枝状硫化银铋的表征

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Nanoparticles and nanostructured dendritic silver bismuth sulfide were successfully produced from silver acetate, bismuth nitrate, and thiosemicarbarzide in ethylene glycol by 140-200°C solvothermal reactions for 24-72 h. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Their SAED patterns were also in accordance with those of the simulations. Scanning and transmission electron microscopies (SEM and TEM) revealed the nanostructured products. Their photoluminescence (PL) emissions were detected at the same wavelength of 380 and 420 nm, although they were produced under different conditions.
机译:纳米粒子和纳米结构树状银硫化铋是由乙酸银,硝酸铋和硫代半碳化物在乙二醇中通过140-200°C溶剂热反应24-72小时成功生产的。使用X射线衍射(XRD)和选定区域电子衍射(SAED)检测相。他们的SAED模式也与模拟的一致。扫描和透射电子显微镜(SEM和TEM)显示出纳米结构的产物。尽管它们是在不同条件下产生的,但在相同的380和420 nm波长下检测到了它们的光致发光(PL)发射。

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