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COMPARISON OF Ag/Bi-2223 TAPES PROCESSED WITH AND WITHOUT HOT-PRESSING AND POST-ANNEALING

机译:有/没有热压和后退火处理的Ag / Bi-2223 TAPES的比较

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Comparative studies on the Ag/Bi-2223 powder-in-tube tapes processed with or without hot pressing and post-annealing were carried out in terms of J_c, J_c-H, and magneto-optical image (MOI). It was found that hot-pressing significantly improved the J_c in zero field. SEM showed that the hot-pressed tapes were highly textured and very dense compared to the tapes without hot pressing. MOI revealed that the current distribution in the hot-pressed tape was more homogeneous than in the cold-pressed tape in the same field. However, there are more pronounced flux penetrations in the former than the latter, suggesting that the hot pressing under a large pressure only improved grain connectivity but not the flux pinning. The pronounced flux penetrations in the hot-pressed tape are attributable to highly stressed grains induced under hot pressing. Although these imperfect grains can carry large critical current in zero field, they broke down and J_c dropped rapidly as soon as a field was applied. By optimising the hot pressing conditions the strain on the oxide core can be largely relieved and J_c-H dependence improved. A post-annealing relieved the strains but created voids, which degraded the connectivity. J_c-H behaviour for the post-annealed tape showed a clear enhancement in weak links in low fields, but an improvement in high fields.
机译:根据J_c,J_c-H和磁光图像(MOI),对经过或不经过热压和后退火处理的Ag / Bi-2223管中粉带进行了比较研究。发现热压显着改善了零场下的J_c。 SEM显示,与没有热压的带相比,热压的带具有高度的织构并且非常致密。 MOI表明,在相同领域中,热压带中的电流分布比冷压带中的电流分布更均匀。但是,前者中的助熔剂渗透要比后者大得多,这表明在大压力下进行热压只会改善晶粒的连通性,而不会改善助熔剂的钉扎作用。热压带中明显的助焊剂渗透归因于在热压下引起的高应力晶粒。尽管这些不完美的晶粒可以在零磁场中承载较大的临界电流,但一旦施加磁场,它们就会击穿并且J_c迅速下降。通过优化热压条件,可以大大减轻氧化物核上的应变,并改善了J_c-H依赖性。后退火缓解了应力,但产生了空隙,从而降低了连接性。后退火磁带的J_c-H行为在弱磁场中显示出明显增强,而在弱磁场中则有所改善。

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