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Study of Thermal Degradation of PVA/Chitosan/Gelatin Electrospun Nanofibers

机译:PVA /壳聚糖/明胶Electrom纳米纤维热降解的研究

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Electrospinning of PVA/Chitosan, PVA/Gelatin, and PVA/Gelatin/Chitosan Blend were prepared to study thermal characteristic by using thermogravimetric analysis (TGA). Electrospinning processes were controlled by applied voltage 16 kVA and tip-to-collector distance (TCD) Of 14 cm. The morphology and structure of the fiber were characterized by using scanning electron microscope (SEM) and Fourier transform infrared (FTIR). The influence of PVA addition showed in an image of SEM. Thermal behavior was showed by comparing thin film of PVA/Gelatin/Chitosan Blend in fiber and dip coating. Thermal stability of these samples showed the different melting temperature and phase transition. Fiber sample indicated to begin earlier at melting temperature than dip coating sample.
机译:制备PVA /壳聚糖,PVA /明胶和PVA /明胶/壳聚糖共混物的静电纺丝,以使用热重分析(TGA)研究热敏性。通过施加的电压16 kVa和尖端到集电极距离(TCD)为14cm的静电纺丝工艺。通过使用扫描电子显微镜(SEM)和傅里叶变换红外(FTIR)来表征光纤的形态和结构。 PVA添加的影响显示在SEM的图像中。通过将PVA /明胶/壳聚糖共混物中的薄膜与纤维和浸涂中的薄膜进行比较来表明热能。这些样品的热稳定性显示出不同的熔融温度和相转变。表示熔融温度较早开始比浸涂样品更早的纤维样品。

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