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A Study on the Atomic Topography of Nanostructured TiO2Thin Films: Effect of Annealing

机译:纳米结构TiO 2 薄膜的原子形貌研究:退火效应

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Titanium dioxide (TiO2) is one of the most investigated metal oxides due to the wide range of applications such as photocatalysts. Photocatalytic activity will increased when the surface area is higher. Hence, this research focus on the surface topography and roughness of nanostructured TiO2films characterized by atomic force microscopy (AFM) in order to obtain thin films with the optimum roughness for photocatalytic activity. TiO2thin films were prepared by spin coating method at room temperature. The TiO2solutions of 0.1–0.2 M were synthesized from titanium butoxide in ethanol. TiO2films were deposited on the silicon substrates and annealed at 450°C. The results shown when the film was annealed, the grain were clearly observed. The grain size and the roughness increased when the film were annealed at high temperature. 0.2 M of TiO2thin film exhibit the higher roughness with Ra and RMS values were 51.29 and 78.90 nm, respectively.
机译:二氧化钛(TiO 2 由于光催化剂的应用范围很广,因此)是研究最多的金属氧化物之一。当表面积较高时,光催化活性将增加。因此,本研究着眼于纳米结构TiO的表面形貌和粗糙度 2 以原子力显微镜(AFM)为特征的薄膜,以获得具有最佳粗糙度的光催化活性薄膜。二氧化钛 2 在室温下通过旋涂法制备薄膜。二氧化钛 2 由丁醇钛在乙醇中合成0.1–0.2 M的溶液。二氧化钛 2 薄膜沉积在硅基板上并在450°C退火。结果表明,当薄膜退火时,可以清楚地观察到晶粒。当薄膜在高温下退火时,晶粒尺寸和粗糙度增加。 TiO 0.2 M 2 薄膜表现出更高的粗糙度,Ra和RMS值分别为51.29和78.90 nm。

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