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Dependence of annealing temperature on microstructure and photoelectrical properties of vanadium oxide thin films prepared by DC reactive sputtering

机译:退火温度对直流反应溅射制备钒氧化物薄膜的微观结构和光电性能的影响

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Vanadium oxide thin films were prepared by DC reactive sputtering method, and the samples were annealed in Ar atmosphere under different temperature for 2 hours. The microstructure, optical and electrical properties of the as-grown and treated samples were characterized by XRD, spectrophotometer, and four-probe technique, respectively. XRD results investigated that the main content of the annealed sample are VO_2 and V_2O_5. With annealing temperature increasing, the intensity of the VO_2 phase diffraction peak strengthened. The electrical properties reveal that the annealed samples exhibit semiconductor-to-metal transition characteristic at about 40°C. Comparison of transmission spectra of the samples at room temperature and 100°C, a drastic drop in IR region is found.
机译:通过DC反应溅射法制备氧化钒薄膜,并在Ar气氛中于不同温度下将样品退火2小时。分别用XRD,分光光度计和四探针技术对生长和处理过的样品的显微结构,光学和电学性质进行了表征。 XRD结果表明,退火后样品的主要含量为VO_2和V_2O_5。随着退火温度的升高,VO_2相衍射峰的强度增强。电学性能表明,退火后的样品在约40°C时表现出从半导体到金属的转变特性。比较样品在室温和100°C下的透射光谱,发现IR区域急剧下降。

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