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Electrospun tin oxide nanofibers with different precursor solution

机译:具有不同前体溶液的静电纺丝氧化锡纳米纤维

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In this paper, electrospinning method was adopted to prepare tin oxide nanofibers membrane with three kinds of novel precursor solution PVP/C_(12)H_(24)O_4Sn, PVP/ G_4H_(10)OSn and PVP/SnCLt. The morphology, surface element, thermal analysis and crystal structure of the fibers membrane were investigated by SEM, EDS, TG-DTA and XRD. The results showed that the organic/inorganic hybrid nanofibers with an average diameter of 300~700 nm can be obtained by electrospinning. But after calcined at 600 °C, the loose and porous tin oxide nanofibers membrane with an average diameter of 100~250 nm can be obtained only by using PVP/SnCU as preceusor solution, moreover, it showed good fiber forming property. From XRD spectra, it was found that the rutile structure tin oxide finally obtained without other crystalline forms.
机译:本文采用静电纺丝法制备了三种新型前驱体溶液PVP / C_(12)H_(24)O_4Sn,PVP / G_4H_(10)OSn和PVP / SnCLt的氧化锡纳米纤维膜。通过SEM,EDS,TG-DTA和XRD对纤维膜的形貌,表面元素,热分析和晶体结构进行了研究。结果表明,电纺丝可以得到平均直径为300〜700 nm的有机/无机杂化纳米纤维。但是在600℃下煅烧后,仅以PVP / SnCU为前驱体溶液就可以得到平均直径为100〜250nm的疏松多孔的氧化锡纳米纤维膜,而且具有良好的成纤性。从XRD光谱发现,最终获得金红石结构的氧化锡而没有其他结晶形式。

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