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Optimization of Processing Parameters for the Ultrasonic Extraction of Geranium

机译:大竺型超声提取处理参数的优化

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A simple and rapid ultrasonic-assisted extraction (UAE) procedure has been developed and optimized for ethanol extraction yield (EEY ) from the Geranium. Several variables that could potentially affect the extraction efficiency, namely, ethanol fraction (%), ultrasonic extracting time (min), liquid.solid ratio (volume per mass) have been optimized by means of response surface methodology (RSM). The optimum conditions were ethanol fraction 66%, liquid.solid ratio (volume per mass) 16:1 and ultrasonic extracting time 64min, Under the optimum operating conditions, the extraction yield was 24.12 %, and UAE showed significantly higher recoveries than those obtained by the conventional extraction methods ( reflux extraction). In addition, a drastic reduction of the ultrasonic extraction time (60 min vs. 8 h) and solvent consumption (16 vs. 30) was achieved, comparable with that provided by the reflux extraction as a reference method.
机译:已经开发了一种简单且快速的超声波辅助提取(UAE)程序,并针对来自Geranium的乙醇提取产率(EEY)进行了优化。几种可能影响提取效率的变量,即乙醇级分(%),超声提取时间(min),液体。通过响应面方法(RSM)优化了液体。液体。液体。最佳条件是乙醇级分66%,液体。溶液比例(每质量体积)16:1和超声波提取时间64min,在最佳的操作条件下,提取产率为24.12%,并且UAE显示出比通过的萃取物显着更高的回收率常规提取方法(回流萃取)。此外,实现超声提取时间(60分钟对8小时)和溶剂消耗(16 vs.30)的急剧减小,与回流萃取作为参考方法提供的。

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