Single Crystal Synthesis of Cubic Garnet Related-type Li_7La_3Zr_2O_(12) by a Self-Flux Method

机译：通过自动助焊法的单晶体合成立方石榴石相关型LI_7LA_3ZR_2O_（12）

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We have successfully synthesized single-crystal samples of fast Li-ion conducting cubic Li_7La_3Zr_2O_(12) with the garnet related-type structure by a self-flux method using LiNO_3 at 1150°C. The as-grown Li_7La_3Zr_2O_(12) crystals are colorless and transparent; they also have a polyhedral-shape with a maximum dimension of 0.15 x 0.10 x 0.10 mm3. The powder XRD pattern shows the obtained crystals have cubic Li_7La_3Zr_2O_(12) structure, and the EDX analysis confirms the chemical composition of La:Zr = 3 :2.

机译：我们已经通过1150℃的LINO_3在1150°C下成功地用石榴石方法合成了快速锂离子传导立方LI_7LA_3ZR_2O_（12）的单晶样本。生长的LI_7LA_3ZR_2O_（12）晶体是无色透明的;它们还具有多面体形状，最大尺寸为0.15×0.10×0.10 mm3。粉末XRD图案显示所获得的晶体具有立方Li_7LA_3ZR_2O_（12）结构，并且EDX分析证实了La：Zr = 3：2的化学成分。

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《Electronics Division Meeting of the Ceramic Society of Japan》|2011年||共4页
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Junji Awaka; Akira Takashima; Hiroshi Hayakawa;
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中图分类 TB3-532;
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Crystal growth; Self-flux method; Lithium-ion conductor; Garnet; Single-crystal X-ray diffraction;

机译：晶体生长;自助法;锂离子导体;石榴石;单晶X射线衍射;

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1. Li Ion Dynamics in Al-Doped Garnet-Type Li_7La_3Zr_2O_(12) Crystallizing with Cubic Symmetry [J] . By Alexander Kuhn, Joon-Yong Choi, Lars Robben Zeitschrift fur Physikalische Chemie: International Journal of Research in Physical Chemistry and Chemical Physics . 2012,第5a6期

机译：Al掺杂石榴石型Li_7La_3Zr_2O_（12）的立方对称结晶锂离子动力学
2. Low-temperature synthesis of Li_7La_3Zr_2O_(12) with cubic garnet-type structure [J] . Hui Xie, Yutao Li, John B. Goodenough Materials Research Bulletin . 2012,第5期

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3. Investigation on Varying Aluminum Doping Concentrations and Sintering Temperatures on the Synthesis of Garnet Li_7La_3Zr_2O_(12) Solid Electrolyte via Modified Pechini Method [J] . Benjamin Jose Alfaro, Rinlee Butch M. Cervera Materials science forum . 2019,第期

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4. Single Crystal Synthesis of Cubic Garnet Related-type Li_7La_3Zr_2O_(12) by a Self-Flux Method [C] . Junji Awaka, Akira Takashima, Hiroshi Hayakawa Electronics Division Meeting of the Ceramic Society of Japan . 2011

机译：通过自动助焊法的单晶体合成立方石榴石相关型LI_7LA_3ZR_2O_（12）
5. Nanofabrication Methods Towards a Photonically-Based Torque Magnetometer for Measurement of Individual Single-Crystalline Yttrium- Iron-Garnet Microstructures [D] . Compton, Shawn R. 2012

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6. Crystal Structure of Garnet-Related Li-Ion ConductorLi7–3xGaxLa3Zr2O12: Fast Li-Ion ConductionCaused by a Different Cubic Modification? [O] . Reinhard Wagner, *, GüntherJ. Redhammer, -1

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7. Single crystal growth by self-flux method of the mixed valence gold halides Cs$_2$[Au$^{I}$X$_2$][Au$^{III}$X$_4$] (X=Br,I) [O] . Riggs, Scott C., Shapiro, M. C., Corredor, F., 2011

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8. Dislocation Barrier Interactions in Cubic Crystals. Volume II. Extended Dislocation Barriers on (112) Planes in Anisotropic Body-Centered Cubic Crystals (Study of the Theory of Phenomena) [R] . Teutonico, L. J. 1967

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Single Crystal Synthesis of Cubic Garnet Related-type Li_7La_3Zr_2O_(12) by a Self-Flux Method

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