首页> 外文会议>Journal of Rare Earths vol.24 Spec. Issue March 2006 >Ferromagnetism of Ni-Doped ZnO Powders Prepared by Sol-Gel Method above Room Temperature
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Ferromagnetism of Ni-Doped ZnO Powders Prepared by Sol-Gel Method above Room Temperature

机译:室温以上Sol-Gel法制备Ni掺杂ZnO粉末的铁磁性

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The magnetic and structural properties of 2% Ni-doped ZnO powers prepared by sol-gel method were studied. X-ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) of the sample do not show existence of any signal of second phase. The X-photoelectron spectroscopy (XPS) of the sample shows the chemical valence of Ni is +2 and the real Ni concentration is 2.19% determined by X-ray fluorescence spectra (XRFS). The magnetic property performed with superconducting quantum interference device (SQUID) shows that the sample exhibits ferromagnetism above room temperature and the Curie temperature ( T_C ) is about 600 K.
机译:研究了溶胶-凝胶法制备的2%掺Ni的ZnO粉末的磁性和结构性能。样品的X射线衍射(XRD)和高分辨率透射电子显微镜(HRTEM)未显示任何第二相信号的存在。样品的X光电子能谱(XPS)显示,Ni的化学价为+2,通过X射线荧光光谱(XRFS)测定的实际Ni浓度为2.19%。用超导量子干涉仪(SQUID)进行的磁性能表明,样品在室温以上表现出铁磁性,居里温度(T_C)约为600 K.

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