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Characterization of Si particles and their effects on and recrystallization in a nanostructured cold rolled Al-1Si alloy

机译:纳米结构冷轧Al-1%Si合金中Si颗粒的表征及其对和再结晶的作用

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An Al-1.08 vol.%Si alloy was cold rolled to a reduction of 98% (ε_(VM) = 4.5) and then annealed at different temperatures up to 210°C (0.52 Tm) for different times. The deformed structure is characterized by a nanoscale lamellar structure with the presence of Si particles of coarse (> 1μm), medium (100 nm - 1 μm) and fine (< 100 nm) sizes in the microstructure. Deformation zones are formed around the coarse Si particles and the boundary spacing is finer in the deformation zone than in the matrix. The medium Si particles have little effect on the morphology and boundary spacing. The fine Si particles are aligned along the lamellar boundaries indicating a stabilizing effect on the structural refinement during cold rolling. After annealing, enhanced recovery occurs in the deformation zones around the coarse Si particles. However the reduction in stored energy during recovery and the pinning effect of fine Si particles on the boundary migration prevent the advantage of particle stimulated nucleation (PSN) of coarse Si particles in the nanoscale lamellar structure. This study also demonstrates an important effect of the fine particles in delaying both recovery and recrystallization processes. This effect diminishes with increasing annealing temperature and coarsening the fine particles especially at triple junctions.
机译:Al-1.08 Vol.%Si合金冷轧至减少98%(ε_(Vm)= 4.5),然后在不同时间的不同温度下退火,不同时间为210℃(0.52吨)。变形结构的特征在于纳米级层状结构,该结构具有粗(>1μm),培养基(100nm - 1μm)和微结构中细(<100nm)尺寸的粗颗粒的存在。围绕粗SI颗粒形成变形区域,并且边界间距在变形区中比在基质中更精细。培养基Si颗粒对形态和边界间距几乎没有影响。细Si颗粒沿着层状边界对齐,表明冷轧过程中对结构细化的稳定作用。退火后,在粗SI颗粒周围的变形区域中发生增强的恢复。然而,在纳米级层状结构中恢复期间储存期间的储存能量和精细Si颗粒的钉扎效应是在纳米级层状结构中的颗粒刺激核颗粒的优点来防止粗Si颗粒的颗粒刺激核(PSN)。该研究还表明了细颗粒在延迟恢复和再结晶过程中的重要作用。这种效果随着退火温度的增加而减少,特别是在三重交叉点处粗化细颗粒。

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