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Microstructural Evolution During High Temperature Deformation of Ti-47Al-2Cr-4Nb intermetallic compound

机译:Ti-47Al-2Cr-4Nb金属间化合物高温变形过程中的组织演变

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The microstructural changes during high temperature deformation behavior of Ti-47Al-2Cr-4Nb intermetallic compound have been ivestigated by isothermal comprssion tests at temperatures ranged 1000-1200 deg C with strain rates ranged 10~(-3) -10~(1-) s~(-1). The stress-strain curve exhibited a peak stress, then the flow stress decreased gradually into a steady state stress with increasing the strain. The flow softening behavior during high temperature deformation is attributed to the dynamic recrystallization. The dependece of flow stress on temperature and strain rate was formulated well using the Zener-Hollomon parameter. The activation energy was measured as 295kJ/mol and the stress exponent was measured as 3.1 for Ti-47Al-2Cr-4Nb. The dynamically recrystallized microstructures were investigated and the relationship between recrystallized grain size and temperature compensated strain rate was discussed. The dynamically recrystallized grain size decreased with decreasing the temperature and increasing the strain rate, while the recrystallization rate increased with increasing the temperature and decrasing the strain rate. The dynamic recrystallization started at the initial grain boundaries and it is suggested that the nucleation of dynamic recrystallization is controlled by the grain boundary migration.
机译:Ti-47Al-2Cr-4Nb金属间化合物高温变形行为期间的微观结构变化已通过等温压缩试验在1000-1200℃的温度范围内以10〜(-3)-10〜(1-)的应变速率进行了研究。 s〜(-1)。应力-应变曲线表现出峰值应力,然后随着应变的增加,流动应力逐渐减小到稳态应力。高温变形过程中的流动软化行为归因于动态再结晶。使用Zener-Hollomon参数可以很好地确定流动应力对温度和应变率的依赖性。 Ti-47Al-2Cr-4Nb的活化能为295kJ / mol,应力指数为3.1。研究了动态再结晶组织,研究了再结晶晶粒尺寸与温度补偿应变率之间的关系。动态再结晶晶粒尺寸随温度降低和应变速率的增加而减小,而再结晶速率随温度升高和应变率的降低而增加。动态再结晶从初始晶界开始,这表明动态再结晶的形核是由晶界迁移控制的。

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