PREPARATION AND CHARACTERIZATION OF IMAZALIL / β-CYCLODEXTRIN INCLUSION COMPLEX BY SUPERCRITICAL CARBON DIOXIDE AND ~(13)C CP-MAS AND ~1H NMR SPECTROSCOPY: PRELIMINARY RESULTS

机译：超临界二氧化碳和〜（13）C CP-MAS和〜1H NMR光谱法制备并表征咪唑/β-环糊精包合物：初步结果

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Imazalil, a selected fungicide, was inclused into β-cyclodextrin using supercritical carbon dioxide. The best experimental conditions were determined to prepare the insertion complex, which was investigated by means of ~1H NMR in aqueous solution and ~(13)C CP-MAS NMR in the solid state. A comparative analysis of the spectra of the free βCD, IMZ and βCD-IMZ gave information on structural properties of the βCD-IMZ complex.

机译：使用超临界二氧化碳将一种精选的杀菌剂Imazalil包含在β-环糊精中。确定了最佳的制备条件，以制备插入配合物，并通过〜1H NMR水溶液和〜（13）C CP-MAS NMR固态进行了研究。游离βCD，IMZ和βCD-IMZ光谱的比较分析提供了有关βCD-IMZ复合物的结构性质的信息。

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来源
《International Symposium on Supercritical Fluids Tome 3: Materials Processing; 20030428-20030430; Versailles; FR》|2003年|P.1903-1910|共8页
会议地点 Versailles(FR)
作者
Marongiu B.; Piras A.; Porcedda S.; Lai A; Lai S.;
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Dipartimento di Scienze Chimiche, Universita di Cagliari, Cittadella Universitaria di Monserrato, 09042 Cagliari, Italy;

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正文语种 eng
中图分类凝聚状态与相变;
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入库时间 2022-08-26 14:19:24

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1. Imazalil-cyclomaltoheptaose (beta-cyclodextrin)inclusion complex:preparation by supercritical carbon dioxide and ~13C CPMAS and ~1H NMR characterization [J] . Simona Lai, Imazalil-cyclomaltoheptaose (beta-cyclodextrin)inclusion complex:preparation by supercritical carbon dioxide and ~13C CPMAS and ~1H NMR characterization, Emanuela Locci, Carbohydrate research . 2003,第21期

机译：Imazalil-cyclomaltoheptaose（β-环糊精）包容复合物：通过超临界二氧化碳和〜13C CPMAS和〜1H NMR表征制备
2. Structural characterization and diffusional analysis of the inclusion complexes of fluoroadamantane with β-cyclodextrin and its derivatives studied via ~1H, ~(13)C and ~(19)F NMR spectroscopy [J] . Xiaojie Gu, Errol V. Mathias, Kim Trang Huu Nguyen Journal of Inclusion Phenomena and Macrocyclic Chemistry . 2013,第3a4期

机译：通过〜1H，〜（13）C和〜（19）F NMR光谱研究氟金刚烷与β-环糊精及其衍生物的包合物的结构表征和扩散分析
3. C-13-CPMAS and H-1-NMR study of the inclusion complexes of beta-cyclodextrin with carvacrol, thymol, and eugenol prepared in supercritical carbon dioxide [J] . Locci E, Lai SM, Piras A, Chemistry & biodiversity . 2004,第9期

机译：超临界二氧化碳中β-环糊精与香芹酚，百里酚和丁香酚的包合物的C-13-CPMAS和H-1-NMR研究
4. ~(13)C CPMAS AND ~1H NMR STUDY OF THE INCLUSION COMPLEXES OF β-CYCLODEXTRIN WITH CARVACROL, THYMOL AND EUGENOL PREPARED BY SUPERCRITICAL CARBON DIOXIDE [C] . Marongiu B., Piras A., Porcedda S., Italian Conference on Supercritical Fluids and Their Applications . 2004

机译：〜（13）C CPMAS和〜1H NMR通过超临界二氧化碳制备的β-环糊精β-环糊精含有β-环糊精的含量复合物
5. Solid-state carbon-13-NMR investigation of di- and tri-block biodegradable copolymers isolated in their inclusion compounds with cyclodextrin. [D] . Porbeni, Francis Ebikefe. 2003

机译：固态碳13核磁共振研究的二嵌段和三嵌段可生物降解的共聚物分离与环糊精的包合物中。
6. Oral bioavailability in pigs of a miconazole/Hydroxypropyl-γ-cyclodextrin/ L-tataric acid inclusion complex produced by supercritical carbon dioxide processing [O] . Valéry Barillaro, Brigitte Evrard, Luc Delattre, 2005

机译：超临界二氧化碳处理产生的咪康唑/羟丙基-γ-环糊精/ L-酒石酸包合物在猪中的口服生物利用度
7. Preparation of Inclusion Complex of Piroxicam with Cyclodextrin by Using Supercritical Carbon Dioxide [O] . Martial Sauceau, Elisabeth Rodier, Jacques Fages 2009

机译：超临界二氧化碳制备吡罗昔康与环糊精包合物
8. Characterization of Plasma Polymerized Hydrocarbons Using CP-MAS Carbon-13 NMR [R] . Gambogi, R. J., Cho, D. L., Yasuda, H., 1991

机译：使用Cp-mas碳-13NmR表征等离子体聚合的烃

PREPARATION AND CHARACTERIZATION OF IMAZALIL / β-CYCLODEXTRIN INCLUSION COMPLEX BY SUPERCRITICAL CARBON DIOXIDE AND ~(13)C CP-MAS AND ~1H NMR SPECTROSCOPY: PRELIMINARY RESULTS

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