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Influence of Synthesis Conditions on the Properties of Nanoparticles and Core/Shell Structures Based on Fe3O4

机译:合成条件对基于Fe 3 O 4 的纳米粒子和核/壳结构性能的影响

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Nanoparticles of ferromagnetic materials were synthesized by different approaches such us co-precipitation from nonaqueous solutions method, cryochemical way and microemulsion technique. In order to obtain core/shell particles, the as-prepared Fe3O4 nanoparticles were covered by CoFe2O4-shell with various thickness. The obtained particles were characterized by powder X-ray diffraction, transmission electron microscopy (TEM), quantum design vibrating sample magnetometer and Mössbauer spectrometry.
机译:采用非水溶液共沉淀法,冷冻化学法和微乳化法等多种方法合成了铁磁材料的纳米粒子。为了获得核/壳颗粒,将所制备的Fe 3 O 4纳米颗粒用具有各种厚度的CoFe 2 O 4-壳覆盖。通过粉末X射线衍射,透射电子显微镜(TEM),量子设计振动样品磁力计和Mössbauer光谱法对获得的颗粒进行表征。

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