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The relationship between dielectric properties and the preparation method of nano-SiO2/epoxy composite

机译:介电性质与纳米SiO 2 /环氧树脂复合材料制备方法的关系

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In this paper, the effect of preparation method on the permittivity and dielectric loss of nano-SiO/epoxy composites was studied. The nano-SiO was dispersed into epoxy resin by three methods, which were “Ultrasonic Dispersion Method”, “High-speed Mixer Method” and “Sol-gel method”. The composites with 1wt%, 2wt%, 3wt% and 4wt% loading were made respectively. To compare the influence of the preparation methods to the permittivity and dielectric loss characteristics, dielectric spectra of the nanocomposites at the frequency range of 10-10 Hz were measured by Novo-control system. The results showed that the permittivity of nanocomposites made by the “High-speed Mixer Method” is lower than that made by the other methods. With the loading of nano-SiO increased, the permittivity of nanocomposites increased then decreased, and reached its maximum at the 3wt% loading. The dielectric loss of nanocomposites is higher than the pure epoxy resin when the frequency is under 1 kHz and as the frequency exceeds 1 kHz, the dielectric loss of the nanocomposites is lower than the pure epoxy resin.
机译:本文研究了制备方法对纳米SiO /环氧树脂复合材料介电常数和介电损耗的影响。通过“超声分散法”,“高速混合器法”和“溶胶-凝胶法”三种方法将纳米二氧化硅分散在环氧树脂中。分别制备了具有1wt%,2wt%,3wt%和4wt%负载的复合材料。为了比较制备方法对介电常数和介电损耗特性的影响,采用Novo控制系统在10-10 Hz的频率范围内测量了纳米复合材料的介电谱。结果表明,“高速混合法”制得的纳米复合材料的介电常数低于其他方法。随着纳米SiO含量的增加,纳米复合材料的介电常数先升高后降低,并在3wt%的载荷下达到最大值。当频率低于1kHz时,纳米复合材料的介电损耗高于纯环氧树脂,并且当频率超过1kHz时,纳米复合材料的介电损耗低于纯环氧树脂。

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