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Structural and morphological features of sol-gel processed pure and Indium doped ZnO nanoparticles

机译:溶胶-凝胶处理的纯铟掺杂ZnO纳米粒子的结构和形态特征

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High purity ZnO nano particles and Indium (In) doped Zinc oxide (ZnO) nano particles were synthesized by simple sol-gel technique at low temperature of 70°C. Different compositions of Indium (In) doped zinc oxide with Zn1−xInxO (x=0.01 to 0.08 atomic percent) were prepared by low cost sol-gel technique. The powders were examined for their structural study using XRD. It has been found from diffraction data that the pure and Indium doped powders have formed to be single phase hexagonal wurtzite crystal structure. The microcstrutured parameters such as strain, lattice constant, particle size, dislocation density, bond lengths between Zn and O were calculated. Using the calculated values of particle size from XRD & SEM crystallinity index was estimated. From the observed crystallinity index data of the prepared nano materials it was confirmed that the materials were showing polycrystalline nature.
机译:通过简单的溶胶-凝胶技术在70°C的低温下合成了高纯度ZnO纳米颗粒和铟(In)掺杂的氧化锌(ZnO)纳米颗粒。通过低成本的溶胶-凝胶技术制备了不同组成的掺有Zn 1-x In x O(x = 0.01至0.08原子百分比)的铟(In)氧化物。使用XRD检查粉末的结构研究。从衍射数据已经发现,纯的和铟掺杂的粉末已经形成为单相六方纤锌矿晶体结构。计算了诸如应变,晶格常数,粒度,位错密度,Zn和O之间的键长之类的微结构参数。使用从XRD和SEM得出的粒径计算值,可以估算结晶度。从所制备的纳米材料的观察到的结晶度指数数据,证实该材料显示出多晶性质。

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