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Analysis method of insulating particles using electrochemical analysis in high concentration redox active electrolyte solution

机译:高浓度氧化还原活性电解质溶液中使用电化学分析绝缘颗粒的分析方法

摘要

The present invention relates to an analysis method using electrochemical analysis, and more particularly, to a method comprising: injecting insulating particles into a reaction solution of an electrochemical cell containing a redox mediator; and an electrochemical analysis method and a reactor comprising the step of measuring a change in current of the electrochemical cell; and a reaction solution; wherein the reactor includes a counter electrode, a reference electrode, and a working electrode having a maximum diagonal length of 1 to 500 μm on the electrode surface, and the reaction solution contains a redox species, , It is characterized in that at least one selected from the group consisting of size, velocity, attractive force, and charge analysis of the insulating particles is measured through the change in the intensity of the current generated when the insulating particles in the reactor collide or adsorb to the surface of the working electrode. An electrochemical analysis kit is provided. When insulating particles are analyzed through the analysis method and analysis kit of the present invention, the measurement sensitivity can be more remarkably increased, and the measurement accuracy of the size of the insulating particles, the access speed to the electrode, the attractive force with the electrode, and the particle surface charge can be improved. can
机译:本发明涉及使用电化学分析的分析方法,更具体地,涉及一种方法,更具体地,涉及一种方法,其包含:将绝缘颗粒注入含有氧化还原介体的电化学电池的反应溶液中;和电化学分析方法和反应器,包括测量电化学电池电流变化的步骤;和反应溶液;其中反应器包括对电极,参考电极和在电极表面上具有1至500μm的最大对角线长度的工作电极,反应溶液含有氧化还原物种,其特征在于至少一种选定的从由大小,速度,有吸引力和绝缘颗粒的电荷分析组成的组通过当反应器中的绝缘颗粒碰撞或吸附到工作电极的表面时产生的电流强度的变化来测量。提供了一种电化学分析试剂盒。当通过本发明的分析方法和分析试剂盒分析绝缘颗粒时,测量灵敏度可以更显着地增加,并且绝缘颗粒的尺寸的测量精度,电极到电极的接入速度,具有吸引力电极和颗粒表面电荷可以提高。能够

著录项

  • 公开/公告号KR20210141851A

    专利类型

  • 公开/公告日2021-11-23

    原文格式PDF

  • 申请/专利权人 한양대학교 산학협력단;

    申请/专利号KR20200057617

  • 发明设计人 장진호;정희정;

    申请日2020-05-14

  • 分类号G01N27/416;G01N27/28;G01N27/403;G01N27/42;

  • 国家 KR

  • 入库时间 2022-08-24 22:31:25

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