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- Production method of silver particles and carbon nano material composite using Couette-Taylor reactor

机译:- 使用Coute-Taylor反应器的银颗粒和碳纳米材料复合材料的制造方法

摘要

The present invention comprises: an outer cylinder, an inner cylinder installed along the same axis as the outer cylinder, and a motor for rotationally driving the inner cylinder; In the method for producing a silver particle and carbon nanomaterial composite using a Couette-Taylor reactor including an inlet and an outlet connected to the external cylinder, the carbon nanomaterial is surface-modified to introduce a functional group into the conductive carbon nanomaterial. making; introducing a functional group capable of reacting with a silver salt precursor into the carbon nanomaterial by mixing the surface-modified carbon nanomaterial with an isocyanate-based compound and a pyrimidine-based compound; injecting the carbon nanomaterial into which the functional group is introduced together with a solvent into the inlet of the Couet-Taylor reactor; injecting the silver salt precursor together with a solvent into the inlet at a constant speed while rotating the inner cylinder; Injecting a reducing agent into the inlet at a constant speed, and forming a Kuwet-Taylor flow through the rotational driving of the inner cylinder to form silver particles of a uniform diameter. Thereby, it is possible to obtain the effect that the carbon nanomaterial, the silver precursor, and the reducing agent are synthesized into silver particles having a uniform diameter by the Kuett-Taylor flow.
机译:本发明包括:外筒,沿与外筒的相同轴安装的内圆筒,以及用于旋转驱动内筒的电动机;在使用包括入口和连接到外筒的出口的豆蛋白反应器的制造银颗粒和碳纳米材料复合物的方法中,表面改性碳纳米材料将官能团引入导电碳纳米材料中。制作;通过将表面改性的碳纳米材料与基于异氰酸酯的化合物和嘧啶的化合物混合,引入能够与银盐前体与银盐前体反应的官能团。用溶剂引入官能团的碳纳米材料进入Couet-Taylor反应器的入口;在旋转内筒的同时将银盐前体与溶剂以恒定速度注入入口;以恒定速度将还原剂注入入口,并通过内圆柱的旋转驱动形成Kuwet-Taylor流,以形成均匀直径的银颗粒。由此,可以获得碳纳米材料,银前体和还原剂的效果合成成具有Kuett-taylor流的均匀直径的银颗粒。

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