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Batch distillation methods, stills, and kits

机译:批量蒸馏方法,剧照和套件

摘要

A method of batch distilling including providing a first substrate that upon distillation releases vapour having deleterious sulfur compounds, providing an inert still, adding the first substrate to the still, installing at least one first reactive article in the still and subsequently performing a first distillation run on the first substrate, such that the installed at least one first reactive article has a first exposed area that is exposed to the distillate, and collecting a first desired fraction from the first run. The distillation during the collection of the first desired fraction is performed at a rate of less than 5 L/(hr*m2) of collected first fraction per first exposed area. Compatible still and kit are also provided.
机译:一种批量蒸馏方法,包括提供第一基板,其在蒸馏后,蒸馏在具有有害硫化合物的蒸汽上,提供惰性的静止,将第一基板添加到静止,在静止中安装至少一个第一反应物品并随后进行第一蒸馏运行 在第一基板上,使得安装的至少一个第一反应性制品具有暴露于馏出物的第一暴露区域,并从第一运行中收集第一所需级分。 在每个第一个暴露区域的第一馏分的收集的第一馏分的速率小于5L /(HR * M2)的速率下进行蒸馏。 还提供兼容套件和套件。

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