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Selenium-doped MXene material, and preparation method and use thereof

机译:硒掺杂的MxENE材料,以及制备方法及其用途

摘要

The present invention discloses a selenium-doped MXene material and a preparation method thereof, comprising the following steps: (1) adding MXene and an organic selenium source into a dispersant, and stirring to prepare a dispersion with a concentration of 10 mg/ml to 100 mg/ml, wherein a mass ratio of MXene and an organic selenium source is 0.1 to 1:1; (2) transferring the dispersion into a reaction kettle, heating to 110° C. to 230° C., reacting for 10 h to 30 h, and then naturally cooling to a room temperature; and (3) washing the product obtained in the step (2) with a cleaning agent, centrifuging to collect a precipitate, and drying the precipitate under vacuum to obtain the selenium-doped MXene material. The composite material prepared by the present invention has high specific surface area, good electrical conductivity, cycle stability performance, rate performance and high theoretical specific capacity.
机译:本发明公开了硒掺杂的偏苯基材料及其制备方法,包括以下步骤:(1)将M烯烃和有机硒源加入分散剂中,并搅拌以制备浓度为10mg / ml的分散体100mg / ml,其中mxene和有机硒源的质量比为0.1至1:1; (2)将分散体转移到反应釜中,加热至110℃至230℃,使10小时至30小时,然后自然地冷却至室温; (3)用清洁剂洗涤在步骤(2)中获得的产物,离心以收集沉淀物,并在真空下干燥沉淀物,得到硒掺杂的偏烯材料。本发明制备的复合材料具有高比表面积,良好的导电性,循环稳定性性能,速率性能和高理论特异性。

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