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Sample injection on gas chromatographs - using pressure regulated purge on injection chamber

机译:在气相色谱仪上进样-在进样室上使用压力调节吹扫

摘要

Gas chromatograph has an input seal for injecting samples. This consists of an inner chamber into which carrier gas is continuously admitted and an outer chamber which is flushed with purge gas and into which the sample is introduced. The pressure of the purge gas in the outer chamber is controlled either by a relief valve and/or an adjustable pressure reducing valve on the purge gas inlet. The pressure reducing valve can be by passed by an on/off valve. For use with gas phase chromatographic analysis of liquid samples. Generally the purge gas chamber is at a higher pressure than the inner chamber and when the sample is injected, a pressure surge enters the column and can upset it. This method avoids such a surge.
机译:气相色谱仪具有用于进样的输入密封件。它由一个内部腔室和一个外部腔室组成,该内部腔室连续容纳载气,该外部腔室被吹扫气体冲洗并引入样品。外室中吹扫气体的压力由吹扫气体入口上的溢流阀和/或可调减压阀控制。减压阀可以通过开/关阀。用于液体样品的气相色谱分析。通常,吹扫气体腔室的压力高于内腔室的压力,并且在注入样品时,压力突波进入色谱柱并使色谱柱不稳。这种方法避免了这种激增。

著录项

  • 公开/公告号DE2530879A1

    专利类型

  • 公开/公告日1976-01-29

    原文格式PDF

  • 申请/专利权人 CIBA-GEIGY AG BASEL (SCHWEIZ);

    申请/专利号DE19752530879

  • 发明设计人 BUSER HANSUELI ARLESHEIM (SCHWEIZ);

    申请日1975-07-10

  • 分类号B01D53/04;G01N31/08;

  • 国家 DE

  • 入库时间 2022-08-23 02:00:21

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