首页> 外国专利> Liquid sample injection pot for gas phase chromatographs - having tangential carrier gas entry and volume sufficient to limit pressure rise on vaporisation to three times initial pressure

Liquid sample injection pot for gas phase chromatographs - having tangential carrier gas entry and volume sufficient to limit pressure rise on vaporisation to three times initial pressure

机译:用于气相色谱仪的液体样品注入罐-具有切向进样气体入口和体积,足以将蒸发时的压力上升限制到初始压力的三倍

摘要

Gas chromatograph sample inlet consists of a tubular body into which the liq. samples are injected. One end is sealed tightly onto the column while the other end has a serum cap seal through which the sample is injected from a syringe. The carrier gas enters from a tangential inlet on the side. The dia. of the evaporation space corresponds at a minimum to the inner dia. of the column. Tge vol. of the injection zone is such that the pressure surge caused by the evaporation of the injected sample is pref. between 2 and 3 times (at most 4 times) the initial pressure. Appts. pref. includes a PTFE flow channel between the evapn. space and the column inlet. For use on gas chromatographs analysing liquid samples. Reduces the mechanical stress on the inlet section and on the column so that the peaks obtained are much closer to the Gaussian function.
机译:气相色谱仪样品入口由一个管状体组成,液体注入其中。样品被注入。一端紧密密封在色谱柱上,而另一端则具有血清盖密封件,可通过该盖从注射器中注入样品。载气从侧面的切向入口进入。直径蒸发空间的最小值至少等于内径。列的。 TGE第一卷进样区的最大压力是这样的,即由进样样品的蒸发引起的压力波动是最佳的。在初始压力​​的2到3倍(最多4倍)之间。 Appts。偏好包括在蒸发之间的PTFE流道。空间和色谱柱入口。适用于分析液体样品的气相色谱仪。降低入口部分和色谱柱上的机械应力,使获得的峰更接近于高斯函数。

著录项

  • 公开/公告号DE2842991A1

    专利类型

  • 公开/公告日1980-04-10

    原文格式PDF

  • 申请/专利权人 GIEGERHANS JOACHIM;

    申请/专利号DE19782842991

  • 发明设计人 JOACHIM GIEGERHANS;

    申请日1978-10-02

  • 分类号G01N31/08;B01D53/04;

  • 国家 DE

  • 入库时间 2022-08-22 17:35:13

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