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High tensile strength, high Young's modulus carbon fiber having excellent internal structure homogeneity, and process for producing the same

机译:具有优异内部结构均质性的高拉伸强度,高杨氏模量的碳纤维及其制造方法

摘要

High tensile strength, high Young's modulus carbon fiber, free from holes and voids having a statistical probability of holes detected by a standard plasma etching test of less than about 2%, a tensile strength of at least about 150 kg/mm.sup.2 and a Young's modulus of at least about 15 × 10.sup.3 kg/mm.sup.2. The carbon fiber has excellent homogeneity of internal structure and excellent reliability as a composite material. PPA process is provided for producing a high performance, high quality carbon fiber having excellent productivity and operability and requiring only a short time for oxidation. The process comprises converting an organic polymeric fiber (preferably an acrylic fiber) to an oxidized fiber, comprising repeatedly bringing said fiber into contact with the surface of a heated body such as a heated roll or heated plate at about 200° - 400° C in the presence of an oxidizing gas for a contact time per single contact of said fiber with the surface of the heated body of less than about 1 second, and heating the resulting oxidized fiber in an atmosphere of an inert gas at a temperature of at least about 800° C to thereby convert the oxidized fiber to a carbon fiber.
机译:高抗张强度,高杨氏模量碳纤维,无孔和空隙,其通过标准等离子体蚀刻测试检测到的孔统计概率小于约2%,抗拉强度至少约为150 kg / mm 2杨氏模量至少约为15×10≤3 kg / mm 2。碳纤维具有优异的内部结构均匀性和作为复合材料的优异的可靠性。

提供了一种用于生产高性能,高质量碳纤维的方法,该碳纤维具有优异的生产率和可操作性,并且仅需要很短的氧化时间。该方法包括将有机聚合物纤维(优选丙烯酸纤维)转化为氧化纤维,包括在大约200℃至400℃下反复使所述纤维与加热体例如加热辊或加热板的表面接触。所述纤维与加热体表面的每次单次接触时间中存在氧化气体的时间少于约1秒,并在惰性气体气氛中将所得氧化纤维在至少约25℃的温度下加热800℃从而将氧化纤维转化为碳纤维。

著录项

  • 公开/公告号US4065549A

    专利类型

  • 公开/公告日1977-12-27

    原文格式PDF

  • 申请/专利权人 TORAY INDUSTRIES INC.;

    申请/专利号US19760713629

  • 发明设计人 YOSHIRO KINOSHITA;

    申请日1976-08-12

  • 分类号D01F9/14;D01F9/22;

  • 国家 US

  • 入库时间 2022-08-22 21:33:37

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