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Process for producing a high tensile strength, high Young's modulus carbon fiber having excellent internal structure homogeneity

机译:具有优异内部结构均匀性的高拉伸强度,高杨氏模量碳纤维的生产方法

摘要

High tensile strength, high Young's modulus carbon fiber, free from holes and voids having a statistical probability of holes detected by a standard plasma etching test of less than about 2%, a tensile strength of at least about 150 kg/mm.sup.2 and a Young's modulus of at least about 15. times.10.sup.3 kg/mm.sup.2. The carbon fiber has excellent homogeneity of internal structure and excellent reliability as a composite material. PPA process is provided for producing a high performance, high quality carbon fiber having excellent productivity and operability and requiring only a short time for oxidation. The process comprises converting an organic polymeric fiber (preferably an acrylic fiber) to an oxidized fiber, comprising repeatedly bringing said fiber into contact with the surface of a heated body such as a heated roll or heated plate at about 200°-400° C. in the presence of an oxidizing gas for a contact time per single contact of said fiber with the surface of the heated body of less than about 1 second, and heating the resulting oxidized fiber in an atmosphere of an inert gas at a temperature of at least about 800° C. to thereby convert the oxidized fiber to a carbon fiber.
机译:高抗张强度,高杨氏模量碳纤维,无孔和空隙,其通过标准等离子体蚀刻测试检测到的孔的统计概率小于约2%,抗张强度至少约为150 kg / mm 2杨氏模量至少约为15乘以10≤3 kg / mm 2。所述碳纤维具有优异的内部结构均匀性和作为复合材料的优异的可靠性。提供一种用于生产高性能,高质量的碳纤维的方法,所述碳纤维具有优异的生产率和可操作性,并且仅需要短时间进行氧化。该方法包括将有机聚合物纤维(优选丙烯酸纤维)转化为氧化纤维,包括使所述纤维与约200°-400℃的加热体如加热辊或加热板的表面反复接触。所述纤维与加热体的表面的每次单接触的接触时间小于1秒,并且在惰性气体气氛中,在至少25℃的温度下,在惰性气体气氛中加热所得的氧化纤维。在约800℃的温度下将氧化纤维转化为碳纤维。

著录项

  • 公开/公告号USRE30414E

    专利类型

  • 公开/公告日1980-10-07

    原文格式PDF

  • 申请/专利权人

    申请/专利号US19790037665

  • 发明设计人 YOSHIRO KINOSHITA;

    申请日1979-05-10

  • 分类号D01F9/14;D01F9/22;

  • 国家 US

  • 入库时间 2022-08-22 16:59:47

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