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A method for the isolation of dinitro anthraquinone with a high content of alpha, alpha ′ - dinitro compounds

机译:一种高含量的α,α'-二硝基化合物的二硝基蒽醌的分离方法

摘要

A process for the isolation of mixtures of 1,5-dinitroanthraquinone and 1,8-dinitroanthraquinone which have a high content of alpha , alpha '-dinitroanthraquinones by heating a suspension of the crude dinitroanthraquinone mixture in certain organic liquids at from 60 DEG to 200 DEG C until solution equilibrium has been set up, and separating the undissolved material from the solution. The undissolved material contains more than 90% and as a rule more than 95% by weight of 1,5-dinitroanthraquinone and 1,8-dinitroanthraquinone. The pure mixture of 1,5-dinitroanthraquinone and 1,8-dinitroanthraquinone may be used for the manufacture of dyes.
机译:通过将粗二硝基蒽醌混合物在某些有机液体中的悬浮液加热到60°C至200°C来分离具有高含量α,α'-二硝基蒽醌的1,5-二硝基蒽醌和1,8-二硝基蒽醌的混合物的方法直至溶液平衡建立,并从溶液中分离出未溶解的物质。不溶解的材料包含按重量计大于90%,并且通常按重量计大于95%的1,5-二硝基蒽醌和1,8-二硝基蒽醌。 1,5-二硝基蒽醌和1,8-二硝基蒽醌的纯混合物可用于制造染料。

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