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METHOD FOR EXTRACTING VOLATILE COMPOUNDS WITH SUPERCRITICAL CARBON DIOXIDE, AND COMPOUNDS SO OBTAINED

机译:超临界二氧化碳萃取挥发性化合物的方法及所获化合物

摘要

In the method disclosed, supercritical CO2 gas is percolated through the starting material and becomes laden with extractible compounds. When the percolation pressure reaches a predetermined value, the pressure in the percolation medium is reduced by bringing said medium into a separation region where the volatile compounds are trapped in the dry ice formed. The compounds are recovered in aqueous solution after sublimation of the CO2. According to the invention, the extraction is carried out in the separation region in the presence of a trapping medium capable of retaining the volatile compounds, advantageously a medium sparingly soluble in liquid or supercritical CO2 and capable of dissolving the volatile compounds (glycerol or edible oil) or of complexing them (cyclodextrins). The starting material chosen has a lipid content which is not excessively high (in particular, fruits and derived products). The trapping medium which retains the volatile compounds and the latter, after separation from said medium, are useful as aromas.
机译:在所公开的方法中,超临界CO 2气体渗透穿过起始材料,并充满可提取的化合物。当渗滤压力达到预定值时,通过使渗滤介质进入分离区,在该分离区中将挥发性化合物捕获在形成的干冰中,从而降低渗滤介质中的压力。二氧化碳升华后,将化合物从水溶液中回收。根据本发明,在能够保留挥发性化合物的捕获介质的存在下,在分离区域中进行提取,该捕获介质有利地是微溶于液体或超临界CO 2并能够溶解挥发性化合物(甘油或食用油)的介质。 )或使其复杂化(环糊精)。选择的起始原料的脂质含量不会过高(特别是水果和衍生产品)。保留挥发性化合物的捕获介质,在与所述介质分离后,将其用作香气。

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